Freeport NIP(7.6)-LR010522'Certes
(.~m~ronmental Laboratories, L.LC.
2~d9 Wisconsin Street, Suite 200
Dallas, Texas 75229
972.620-7966
972.620-7963 FAX · Email: alasalle~certeslabs, com
CERTES fNVIRONMENTAL LABORATORIES
File Number: 01-1456
Prepared for:
P.O. BOX 129
Le~s~He, ~ 75067
' 05/22/01
of chemical analyses for the samples submitted to Certes Environmental
Laboratories, L.L.C., on 05/18/01. All analytical results meet Quality Control requirements as set by the
industry accepted criteria. Please refer to the Laboratory Quality Consol Results section of this report.
This report must be reproduced in its entirety.
Sincerely,
Certes Environmental Laboratories, L.L.C.
Amy LaSalle
President
Analytical Chemistry Environmental Sciences Research Microbiology
May 23, 2001
CASE NARRATIVE
01-1456
Metroplex Underground LP
SamPles for Certes fileI ~r_01f14_56 were ~ceived at the laboratory on 05/18/01. These
samples were analyze~ total ColifoVgM9132. ~
During the analysis of C~ les batch T~a~YS~otal Coliform by SM 91 ]~kno eolonie~
were found above the rep, !i~ln~&~'~~e~ort. Therefore, Fecal Coli~a, a
(972) 620-7966 if you have any questions.
Sincerely,
Tracy~Ma den~~
Project Manager
Certes Environmental Laboratories L. L. C.
Certes Environmental Laboratories, LLC.
2209 Wisconsin Street, Suite EO0 · Dallas. Texas ?~9 · 972-620-7966 · 972-620-7963 FAX
Analytical Chemistry Environmental Sciences F~ese_arch Microbiology
· Results of Analyses CEL File No.: 01-1456 Report Date: 05/22/01
Reporting Date Date Analyzed
Result Units Limit Prepared Analyzed Flag By Dilution
Client Sample ID: 7+32 Sample Number: 01-1456-001
Date Sampled: 05/18/01
Time Sampled: I ~ ~ Sampled ~ample Matrix: Liquid By:
SM 9132 Total Coliform < 2 ~ col/100mL 05/18/01 05/19/01 GRD 2
Client Sample ID: 13-H)5 Sample Number: 01-1456-002
Date Sampled: 05/18/01 Sample Matrix: Liquid
Time Sampled: Sampled By:
SM9132 . TotaIColiform < I col/100mL 05/18/01 05/19/01 GRD I
Client Sample ID: 22+91 Sample Number: 01-1456-003
Date Sampled: 05/10/01 Sample Matrix: Liquid
Time Sampled: Sampled By:
SM 9132 Total Coliform < 1 col/100m] 05/18/01 05/19/01 GRD 1
Client Sample ID: 32+00 Sample Number: 01-1456-004
Date Sampled: 05/18/01 Sample Matrix: Liquid
Time Sampled: Sampled By:
SM 9132 Total Coliform < 1 col/10om] 05/18/01 05/19/01 GRD I
Page 2 of 3
CeAes Environmental Labomlor~s, L.LC.
2209 Wisconsin Street, Suite 200 · Dallas, Texas 75229 * 972-620-7966 · 972-620-7963 FAX
Analytical Chemistry Environmental Sciences Research Microbiology
i Index of Narrative Footnotes
IA - Sample received with headspace for volatile analysis.
B - Analyte detected in the associated method blank.
C - Sample received in unapproved containers.
D - Smxogate diluted out of range.
DNI - Sample does not ignite.
- Result is above the linear range of the instrument and is to be considered an estimate.
H - Sample contains significant levels of heavy petroleum products > C28.
[ - Sample was reported at a dilution with few or no reportable values as a result of matrix interference.
- Value is a J-value and to be considered an estimate only.
L - Re-analysis was not possible due to limited sample amount.
Vi - Recoveries out of range due to matrix interferences inherent in sample.
- Sample has presumptive compounds other than fuel products.
Nj. The analysis indicates the presence of an analyte that has been "tentatively identified" and the associated
numerical value represents its approximate concentration.
- Sample received out of hold time.
? - Result is unconfirmed. The quantitative result from the primary column and secondary column did not agree
within 40%.
R - The sample results are rejected due to serious deficiencies in the ability to analyze the sample and meet quality
control criteria. The presence or absence oftbe analyte cannot be verified.
RR - Sample being re-extracted due to failing surrogate or internal standard.
- Analysis performed at subcontract laboratory.
T - Sample prepared or analyzed out of hold time.
U - The analyte was analyzed for, but was not detected above the reported sample quantitation limit.
UJ - The anaiyte was not detected above the reported sample quantitation limit. However, the reported quantitation
limit is approximate and may or may not represent the actual limit of quantitation neeassary to accurately and
precisely measure the analyte in the sample.
V - Insufficient sample was available for analysis as prescribed by the method. The lesser amount used for analysis
raised reporting limits accordingly.
K - Laboratory contamination suspected.
Y - Benzo(B) and Benzo(K) Fluoranthene did not resolve. Value was reported as Benzo(B)fluoranthene.
g - Dilution was required due to the dark color and thickness of the extract.
- Analytical result reported on dry weight basis.
Page 3 of 3
Certes Environmental Laboratodes, LLC.
2209 Wisconsin Street, Suite 200 · Dallas, Texas 75229 · 972-620-7966 * 972-620-7963 FAX
Analytical Chemistry Environmental Sciences Research Microbiology
Results of Analyses = Laboratory Quality Control
File No.: 01=1456
Duplicate
Batch Number TC-051801
Date Prepared 05/I 8/01
Date Analyzed 05/18/01
Spiked Sample ID 1456-1
Sample Result <2.00
Sam?lc Duplicate Result <2.00
Relative Percent Diffe~nce (RPD) 0
RPD % Control Limits (low-high) 0-20
% Rec. Control Limits (low-high) 85-115
Method Blank N/A
Laboratory Control Sample
Spike Level N/A
Spike Result N/A
% Recovery N/A
Spike Duplicate Result N/A
Recovery Duplicate
N/A
Relative Percent Difference (RPD) N/A
RPD % Control Limits (Iow-high) N/A
% Rec. Control Limits (low-high) N/A
gg/L = micrograms per liter (ppb)
gg/Kg = micmgram~ per kilogram (ppb)
< = less than
MS = Matrix Spike
MSD = MaUix Spike Duplicate
LCS = Laboratory Control Sample
BS = Bench Spike
gmhos/cm = micromhos/ccntimeter
mg/L = milligrams per liter (ppm)
rog/Kg = milligrams per kilogram (ppm)
% = percent
RPD = Relative Percentage Difference
RW - Reagent Water
LCSD = Laboratory Control Sample Duplicate
BSD = Bench Spike Duplicate
C,~fles Environmental Lat30ratories, LLC.
2209 Wisconsin Street. Suite 200 · Dallas, Texas 75229 · 972-620-7966 · 972-620-7963 FAX
Analytical Chemistry Environmental Sciences Research Microbiology
Turnaround Time: ] Sample Receipt (Laboratory Use Only) Yes No
Cer~e~ 2209 wisconsin Street, Suite 200 Standard- Yes r~ RUSH' Yes r~ I la. Samples ~ 4 degrees Celsius? i
~ Dallas, Texas 75229 · LI · L.I lb. Temporatme of cooler?. ~[~
Environmental Labortturies (972)620-7966 (972)620-7963 If RUSH: II--] 2f-] 31-] $[-] Days? 2. Samples reccivcd intact?. I
. I 3.. ~ hoad~ for vC~ s? ~ ~ -
Company Phone No. Fax No. ] d. Correct containers used? [
.. 5. Adequate volume provided?
¢?2- "'
Contact (Report Redplent) o- What type reporting feature would you like to use? 7. Samples received within homing time? '
~ ~ ........ 8, ^green~mt between COC and sample ]abels?
~e ~'~' ,~'*// -,~: -es u EDp: Yes ,, I Samples Shipped by: UPS FedEx Other
co~ ;.p..y Addr:~ City Sta,e Zip ] Sample~po=d ~y: ~ C~ Co~,
, . Comments:
BIIIInS Address (If Different) City Slut; ~lp [
[ Analysis(es) R~que;ted (LI~I specific method, if required)
Sampled By Client Prolect ID Site Location [
Relinquished By (Signature): Ihte 'Fane Relinquished B]MC~,nature): Certes Job Number
Rq~ulshod B]M~nature): Date I 'lime Received for I~
_)